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AFM Testing Cases

Module on Atomic Force Microscopy (AFM)

By E. A. Leone

Brief History

  • Scanning Tunneling Microscope (STM)
    • Developed in 1982 by Binning, Rohrer, and Weibel at IBM Zurich,Switzerland
    • Binning and Rohrer won the Nobel Prize in Physics in 1986
  • Atomic Force Microscope (AFM)
    • Developed in 1986 by Binning, Quate, and Gerber, as a collaboration between IBM and Stanford University

Definitions

  • Scanning Probe Microscope (SPM)
    • Family of microscopies where a sharp probe is scanned across a surface and the probe/ sample interactions are monitored
  • There are Two Major Forms of SPM
    1. STM
    2. AFM
  • There are 3 Major forms of AFM
    • Contact Mode AFM
    • Non-Contact mode
    • Tapping Mode

Feedback Loop Electronics

  • Tapping Mode AFM
  • Cantilever oscillates at about 200 kHz with amplitude of about 20-100 nm
  • Feedback is constant RMS amplitude of the Photodiode detector
  • Piezo moves z to obtain topographic image

A number of SPM Probes are Available to use for Nanotechnology Characterization

  • Contact mode AFM
  • Lateral Force
  • TappingMode AFM
  • Non-contact AFM
  • Force-volume imaging
  • Magnetic Force
  • Electric Field
  • Surface Potential
  • Scanning Tunneling Microscopy
  • Operation in fluid
  • Phase Imaging
  • Quadrex3
  • Scanning Capacitance
  • Conductive AFM
  • Nanolithography
  • NanoManipulation
  • 4-point probe
  • NanoIndentation
  • Scanning Spreading resistance
  • Torsional Resosnance Mode

500 Å Metal Oxide on Silicon Wafer

500 Å Metal Oxide on Silicon Wafer

Nano Indentation with AFM

Atomic Force Microscopy (AFM) Analysis – Nano Scratching in Gold

Nano Indentation with AFM

AFM Summary

  • AFM used to observe the surface morphology at high magnifications.
  • Accurate height (roughness) measurements can be made.
  • A large range of “modules” are available to measure a number of surface properties.